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Surprising discoveries in grain boundary structure could advance material durability
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Surprising discoveries in grain boundary structure could advance material durability
by Robert Schreiber
Berlin, Germany (SPX) Oct 30, 2024



Most industrial materials feature a polycrystalline structure, where atoms form a regular lattice within different crystals. These crystals, separated by grain boundaries, vary in orientation. "These grain boundaries have an enormous influence on the durability and overall performance of a material," stated Dr. Vivek Devulapalli, who conducted the microscopy work for the study. He further explained, "But we have very limited understanding what happens when elements segregate to grain boundaries and how they influence the properties of a material."

This research used advanced atomic-resolution scanning transmission electron microscopy in combination with sophisticated simulations to observe and model these grain boundary structures at an atomic level. A specialized algorithm for predicting grain boundary structures enabled researchers to generate experimentally observed structures, leading to a deeper study of these arrangements. "Our simulations show that for different iron contents, we always find the cage structures as the underlying building blocks of different grain boundary phases. As the iron level increases at the grain boundary, more icosahedral units appear and eventually agglomerate," explained Dr. Enze Chen from Stanford University. An icosahedron, a geometric structure with 12 vertices and 20 planes, serves as the base model for these findings.

Dr. Timofey Frolov, who led the computational aspect of the study, added, "We have identified more than five distinct structures or grain boundary phases of the same boundary, all composed of different arrangements of the same icosahedral cage units."

The study uncovered that these icosahedral cage units enable high-density iron packing. "The icosahedral cages enable a dense packing of iron atoms and since they can form aperiodic clusters, more than two to three times the amount of iron can be accommodated at the grain boundary," Devulapalli explained. Dr. Chen added, "It appears as if iron is trapped inside of quasicrystalline-like grain boundary phases." Liebscher noted that further research is needed to understand how these cage properties influence the material's interface and overall behavior.

The research opens doors to novel materials design methods by manipulating the formation of icosahedral grain boundary phases. Future studies aim to explore how these grain boundary states can adjust material functions and enhance resilience against degradation.

Research Report:Topological grain boundary segregation transitions

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